Detailed Investigation of Fluoromethyl 1,1,1,3,3,3-Hexafluoro-2-Propyl Ether (Sevoflurane) and Its Degradation Products. Part II: Two-Dimensional Fluorine-19 NMR Characterization of Fluoromethyl 1,1,3,3,3-Pentafluoro-2-Propenyl Ether

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Abstract:

One- and two-dimensional 19F NMR spectroscopy has been used to elucidate the molecular structure of a novel compound: fluoromethyl 1,1,3,3,3-pentafluoro-2-propenyl ether. A detailed investigation has provided a means of understanding the complex nature of the one-dimensional 19F NMR spectrum of this compound. In addition, J values are used to predict the molecular conformation.

Keywords: 19F, two-dimensional NMR; Molecular structure; NMR; Spectroscopic techniques

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702894202012

Affiliations: 1: The BOC Group, Inc., Technical Center, Murray Hill, New Jersey 07974 2: Anaquest, a division of BOC Health Care, Murray Hill, New Jersey 07974 3: The BOC Group, Inc., Technical Center, Murray Hill, New Jersey 07974; present address: Conaught Labs., Swiftwater, PA

Publication date: January 1, 1989

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