Condensed-Phase Reactions of Vanadium in the Pyrolytic Graphite-Coated Furnace: Analysis by X-Ray Powder Diffraction

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Abstract:

The sequences of solid-phase reactions preceding formation of atomic vapors in the pyrolytic graphite-coated furnace have been inferred from appearance temperatures, activation energies, and multiple-phase high-temperature thermodynamic calculations. Of these, only the latter provides information on the penultimate and earlier steps preceding atom formation.

Keywords: Electrothermal atomic absorption; Vanadium atomization; X-ray powder diffraction

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/0003702884428824

Affiliations: 1: Department of Analytical Chemistry, The University of New South Wales, P.O. Box 1, Kensington, N.S.W. 2033, Australia 2: Department of Chemistry, University of Canterbury, Christchurch 1, New Zealand

Publication date: January 1, 1988

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