Sample Cells for Studies of Catalytic Materials by ESR and NMR Spectroscopies

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Abstract:

We describe the construction of sample cells for ESR and NMR spectroscopy of air-sensitive materials. The cells are designed for repeated exposure of the material to an atmosphere through attachment to a gas manifold, as would occur in studies of sorption onto heterogeneous catalysts and in flow systems.

Keywords: Electron spin resonance, ESR; Nuclear magnetic resonance, NMR, Catalysts; Sample cell

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702874448553

Affiliations: 1: Department of Chemistry, University of Delaware, Newark, Delaware 19716; present address: Agricultural Products Department, E. I. du Pont de Nemours and Company, Inc., Wilmington, DE 19898 2: Department of Chemistry, University of Delaware, Newark, Delaware 19716

Publication date: May 1, 1987

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