Evaluation of Microwave-Induced Air-Plasma as an Excitation Source

Authors: Zhang, Y.K.1; Hanamura, S.2; Winefordner, J.D.2

Source: Applied Spectroscopy, Volume 39, Issue 2, Pages 211-361 (March/April 1985) , pp. 226-230(5)

Publisher: Society for Applied Spectroscopy

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Abstract:

A single-electrode atmospheric pressure microwave discharge air-plasma is reported. Fundamental characteristics, such as the effects of microwave power, auxiliary air flow, and nebulizer air flow on emission intensity, detection limits, and dynamic ranges for twelve elements and several interference experiments are reported. The plasma temperature is found to be about 4700°K. This simple system can be applied to the spectrochemical analysis of solution samples. The results with the use of this system to determine calcium, sodium, and potassium in SRM-1566 (oyster tissue) and SRM-92 (low-boron glass) show excellent agreement with the NBSs certified values.

Keywords: Emission spectroscopy

Document Type: Research article

DOI: http://dx.doi.org/10.1366/0003702854248962

Affiliations: 1: Department of Chemistry, University of Florida, Gainesville, Florida 32611; present address: Shanghai Institute of Ceramics, Academia Sinica, Shanghai 2: Department of Chemistry, University of Florida, Gainesville, Florida 32611

Publication date: 1985-03-01

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