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Calcium Fluoride Anvil Cell for High-Pressure Infrared Spectroscopy

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Abstract:

In many high-pressure vibrational spectroscopic studies the pressure required is below about 10 kbar, Moreover, infrared microanalysis is usually carried out with a diamond anvil cell under a pressure of less than 1 kbar. Therefore, we have recently developed a cheaper and more readily available glass anvil cell for high-pressure Raman and infrared spectroscopies. However, glass strongly absorbs infrared radiation in the frequency region below 2750 cm−1 and thus the glass anvil cell can be used for high-pressure infrared spectroscopy only in the frequency range above 2750 cm−1.

Keywords: High-pressure cell; Infrared spectroscopy

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702844555287

Affiliations: Division of Chemistry, National Research Council of Canada, Ottawa, Ontario K1A 0R6, Canada

Publication date: July 1, 1984

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