The Design and Characterization of an Interface for High Performance Liquid Chromatography with Direct Current Argon Plasma Detection

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Abstract:

The design and characterization of a nebulizer/spray chamber interface for high performance liquid chromatography-direct current argon plasma spectroscopy are presented. Optimum geometry for this interface was determined by the varying of the chimney tip diameter. Mechanical efficiencies of the interface as a function of nebulizer argon flow are tabulated. The particle velocity distribution within the solvent spray created by the nebulizer and emerging from the interface chimney was measured with the use of laser-Doppler anemometry.

Keywords: HPLC-DCP; Laser-Doppler anemometry; Nebulizer/spray chamber interface; Particle velocity

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702844555197

Affiliations: Department of Chemistry, Graduate Research Center Towers, University of Massachusetts, Amherst, Massachusetts 01003-0035

Publication date: July 1, 1984

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