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Spinning Cell for Low Temperature Resonance Raman Spectra without Dewar Losses

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Abstract:

Thermal and photo decomposition, particularly of solid samples, have been chronic problems in the field of resonance Raman spectroscopy due to the absorption by the sample of very intense tightly focused laser light. Strenuous efforts have been made to minimize sample damage by cooling methods as well as by laser beam dispersion. The use of sample spinning cells is also widely practiced in order to increase the time-averaged area of irradiation.

Keywords: Porphyrin complex; Resonance Raman spectroscopy, low temperature; Spinning cell

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702834634505

Affiliations: Department of Chemistry, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139

Publication date: May 1, 1983

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