Diffuse Reflectance UV-VIS Spectroscopy, an Economical Method for Studying Reagents Immobilized on Silica Gel

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Diffuse reflectance UV-VIS spectroscopy is presented as an economical tool for studying reagents immobilized on silica gel. An appropriate approach to eliminating the spectral contribution of the substrate is presented. Diffuse reflectance spectra of the immobilized reagents, presented as the Kubelka-Munk function, are shown to resemble transmission spectra of model compounds. Several applications are presented in which immobilization sequences were monitored.

Keywords: Reflectance spectroscopy; Surface analysis; Visible UV spectroscopy

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702834634587

Affiliations: Department of Chemistry, College of the Holy Cross, Worcester, Massachusetts 01610

Publication date: May 1, 1983

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