Monitoring the Heterogeneous Reaction of LiH and LiOH with H2O and CO2 by Diffuse Reflectance Infrared Fourier Transform Spectroscopy

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Abstract:

Measurement of the reaction of water vapor and carbon dioxide with lithium compounds such as LiH and LiOH has been carried out in situ using diffuse reflectance infrared Fourier transform (DRIFT) Spectroscopy. The bakeable high-vacuum cell, based on a modification of a commercial diffuse reflectance infrared cell is described along with means for controlling the gaseous and thermal environment.

Keywords: Diffuse reflectance; Fourier transform infrared spectroscopy; Heterogeneous reactions; Surface analysis

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/0003702834634280

Affiliations: 1: Plant Laboratory Department, Y-12 Product Certification Division, Oak Ridge Y-12 Plant, Union Carbide Corporation, Oak Ridge, Tennessee 37830 2: Chemical Processes Department, Y-12 Development Division, Oak Ridge Y-12 Plant, Union Carbide Corporation, Oak Ridge, Tennessee 37830

Publication date: January 1, 1983

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