Qualitative and Relative Quantitative Determination of Primary, Secondary, and Tertiary Aliphatic Amines by 1H-NMR

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A simple and relatively fast method for determination of primary, secondary, and tertiary amines by 1H-NMR is described. This method has the advantage of requiring a small amount of sample (15 to 25 mg) and indicating the presence of all three classes of amines in a single 1H-NMR spectrum.

Keywords: 1H-NMR; Aliphatic amines, primary, secondary, and tertiary

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/0003702794925273

Affiliations: Armak Company, Research Laboratory, 8401 W. 47th Street, McCook, Illinois 60525

Publication date: September 1, 1979

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