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Emission Spectrographic Determination of Selected Metals in Magnesium Alloys by the dc Arc-Powder Technique

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A method is presented for the determination of trace quantities of tungsten, tantalum, niobium, molybdenum, vanadium, and chromium in magnesium alloys. In the procedure, the alloys are converted to their sulfates and excited by a 12 A dc are for 70 s in a Harvey Crater graphite electrode. Magnesium sulfate synthetic standards are used. Minimum detectable concentrations ranging from 1 ppm molybdenum and chromium to 20 ppm tungsten and tantalum are indicated. The standard deviations range from 2.9 ppm for tantalum to 9.9 ppm for tungsten at the 50 ppm concentration range.

Keywords: Arc, dc; Emission spectroscopy; Magnesium alloy analysis

Document Type: Research Article


Affiliations: Rolla Metallurgy Research Center, Bureau of Mines, U.S. Department of the Interior, Rolla, Missouri 65401

Publication date: March 1, 1978

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