V, Cr, Mn, Fe, and Ni in TiO2: Determination by Peak Switching Spark-Source Mass Spectroscopy

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Abstract:

Spark-source mass spectrometry using the peak switching mode of electrical detection has been used for the quantitative analysis of V, Cr, Mn, Fe, and Ni in titanium dioxide pigments. Standards of differing histories form linear calibration curves down to 0.4 ppm when a source coldfinger was used to condense hydrocarbon species. An over-all relative standard deviation of 12.7% was obtained for V, Cr, Mn, Fe, and Ni in the TiO2 standards.

Keywords: Peak switching electrical detection; Spark-source mass spectrometry; Trace element analysis

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370273774333425

Affiliations: N L Industries, Inc., Central Research Laboratory, Hightstown, New Jersey 08520

Publication date: July 1, 1973

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