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A Nonbreakable Nuclear Magnetic Resonance Sample Container for Radioactive Materials

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Abstract:

Our organoactinide research efforts have stimulated the development of several sample handling innovations. Of particular interest was the nuclear magnetic resonance spectroscopic investigation of radioactive as well as water- and air-sensitive compounds. The potential for accidental radioactive contamination release by breakage of a standard NMR sample glass tube was considered an unacceptable hazard. To eliminate this potential, a simple nonbreakable sample container was designed for insertion into a standard (5.0 mm o.d.) glass NMR tube. This sample arrangement permitted routine NMR analyses on radioactive materials to be carried out with a minimum risk.

Keywords: Nuclear magnetic resonance; Radioactive sampling; Spectroscopic technique

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370272774351868

Affiliations: Dow Chemical U. S. A., Rocky Flats Division, P.O. Box 888, Golden, Colorado 80401

Publication date: September 1, 1972

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