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A Simple System for Transferring Air-Sensitive Compounds into Capillaries from Schlenk Tubes

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Abstract:

Our organoactinide research has produced a number of extremely air-sensitive compounds. Experimental difficulties have been encountered during the transfer of these air-sensitive compounds from Schlenk tubes into capillary tubes for mass spectral analysis. To overcome these experimental difficulties, a simple transfer device (see Fig. 1) has been designed.

Keywords: Mass spectral analysis; Organoactinides sampling; Spectroscopic technique

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370272774352506

Affiliations: Dow Chemical, Rocky Flats Division, Golden, Colorado 80401

Publication date: January 1, 1972

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