Pulsed NMR Sulfur-33 Investigations with a Superconducting Solenoid

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There is much interest in examining the structure of sulfur compounds because of the role of sulfur as a principal contributor to environmental pollution. By a pulsed NMR technique, the extremely weak free induction decay signal of 33S in several liquid compounds was detected. Using the relatively easy to detect carbon disulfide resonance as a reference model, a method is discussed for studying sulfur compounds which takes into consideration the symmetry and spin relaxation parameters (T 1 and T 2). Consideration is given to the instrumental parameters which can be varied to enhance 33S pulsed NMR resonances.

Keywords: Instrumentation, NMR; NMR Sulfur-33

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370271779949122

Affiliations: 1: U. S. Department of the Interior, Bureau of Mines, Morgantown Energy Research Center, Morgantown, West Virginia 26505 2: Nuclear Magnetic Resonance Specialties, Incorporated, New Kensington, Pennsylvania 15068

Publication date: May 1, 1971

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