A Windowless Cell for Laser–Raman Spectroscopy of Molten Fluorides

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A captive liquid, or windowless cell has been developed for laser–Raman spectroscopy of molten fluorides. This all-metal cell, 7/32 in. o.d. and 1 1/8 in. long, is contained in a 6 mm i.d., 8 mm o.d. quartz tube which has an optical flat fused to one end. There is no direct contact between the fused salt and the quartz container. Cells of this design, constructed either from nickel or copper, have been used for Raman studies of molten fluorides to 800°C.

Keywords: High temperatures; Molten fluorides; Molten salts; Raman cell; Raman spectroscopy

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370271774371092

Affiliations: Oak Ridge National Laboratory, Oak Ridge, Tennessee 37830

Publication date: January 1, 1971

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