Apparatus for the Preparation of Sealed Samples for NMR

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Abstract:

Many times when measuring the NMR spectra of certain compounds it is necessary to protect the sample from atmospheric oxygen or water. The effect of dissolved oxygen on the NMR spectrum is well known. It may also be necessary or desirable to obtain the NMR spectrum with the sample compound in an appropriate solvent together with a reference standard. These considerations are particularly important when obtaining reference spectra of high-purity standard-sample compounds.

Keywords: NMR instrumentation; Sampling tube for NMR

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/000370269774380356

Affiliations: U. S. Department of the Interior, Bureau of Mines, Laramie Petroleum Research Center, Laramie, Wyoming 82070

Publication date: November 1, 1969

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