Method for Rapid Transfer of GLC Fractions into Infrared Cavity Cells

Author: Kendall, R. F.

Source: Applied Spectroscopy, Volume 21, Issue 1, Pages 1-45 (January/February 1967) , pp. 31-32(2)

Publisher: Society for Applied Spectroscopy

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Abstract:

Combining gas-liquid chromatography (GLC) and infrared spectrophotometry is an established analytical practice. Special trapping procedures are required, however, for the collection and successful infrared analysis of microliter samples obtained from GLC instruments. Procedures designed for the collection of volatile GLC effluents include: (1) Trapping in powdered potassium bromide, followed by pelleting; (2) trapping in thermoelectrically cooled cells, for use with multiple reflection attachments; (3) trapping in capillary tubes containing solvent; and (4) trapping through a special fraction collector into ultramicrocavity cells, which are used with beam-condensing equipment.

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/000370267774385407

Affiliations: Bartlesville Petroleum Research Center, Bureau of Mines, U. S. Department of the Interior, Bartlesville, Oklahoma

Publication date: January 1, 1967

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