Quantitative Determination of Carbon in Solid Hydrocarbons Using the Intensity Ratio of Incoherent to Coherent Scattering Of X-Rays

Authors: Toussaint, C. J.; Vos, G.

Source: Applied Spectroscopy, Volume 18, Issue 6, Pages 161-193 (November 1964) , pp. 171-174(4)

Publisher: Society for Applied Spectroscopy

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Abstract:

A method is presented for the determination of carbon in solid hydrocarbons using the intensity ratio of incoherent to coherent scattering of x-rays. The method is very rapid with precision at the 95% confidence level of about ±0.3%. The minimum sample weight necessary is 0.2 g. Analysis of samples by the x-ray method shows good agreement with values obtained by microcombustion. Finally a general comparison between different methods for carbon determination in solid hydrocarbons is discussed.

Document Type: Research Article

DOI: http://dx.doi.org/10.1366/000370264789620295

Affiliations: Chemistry Department, Analytical and Mineral Chemistry Section Euratom, CCR, Ispra, Italy

Publication date: November 1, 1964

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