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Deuteration of Acrylonitrile

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Abstract:

During preparation of acrylonitrile-1-d,

CH2=CHD—CN,

by D2O exchange, as described by Leitch (1), it was found that a linear relationship obtained between absorbance values for the 1165 cm−1 band and the degree of exchange indicated by mass spectrometer data. This note contains a brief description of the exchange experiment, spectra of acrylonitrile before and after deuteration, and a table of IR and mass spectral data recorded at intervals during the exchange.

Document Type: Short Communication

DOI: http://dx.doi.org/10.1366/000370257774633213

Affiliations: Defence Research Chemical Laboratories, Defence Research Board, Ottawa, Ont., Canada

Publication date: November 1, 1957

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