The Determination of Uranium in Solution by X-Ray Spectrometry

Authors: Wilson, Harry M.; Wheeler, G.V.

Source: Applied Spectroscopy, Volume 11, Issue 3, Pages 113-137 (August 1957) , pp. 128-131(4)

Publisher: Society for Applied Spectroscopy

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Abstract:

A rapid, precise method for the determination of uranium in nitric acid solution is presented. The uranium in solution is excited by a primary x-ray beam from a molybdenum tube. The intensity of the uranium Lα1 emission line is measured by means of a crystal spectrometer employing a scintillation counter and pulse height analyzer. This intensity is converted to concentration by relating to standard solutions

The modification of commercial equipment that simplified the solution analysis are described, as are comparisons of various instrument components.

Document Type: Research article

DOI: http://dx.doi.org/10.1366/000370257774633321

Affiliations: 1: Phillips Petroleum Company, Atomic Energy Division, Idaho Falls, Idaho

Publication date: 1957-08-01

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