If you are experiencing problems downloading PDF or HTML fulltext, our helpdesk recommend clearing your browser cache and trying again. If you need help in clearing your cache, please click here . Still need help? Email help@ingentaconnect.com

Use of an air brush to spray dry samples for X-ray powder diffraction

$14.96 plus tax (Refund Policy)

Buy Article:

Abstract:

The construction and operation of a spray drier is described where the spray is produced using an air brush, essentially a miniature spray gun. The spray-dried products consist of spheres 50-60 m in diameter and typical product recoveries are 80%, a marked improvement over simple two-nozzle systems. The spray-dried samples are easy to load into XRD powder holders and present a smooth surface and relatively constant bulk density to the X-ray beam. Problems of preferred orientation are effectively eliminated and the resulting X-ray powder patterns are completely reproducible by different operators.

Document Type: Research Article

DOI: http://dx.doi.org/10.1180/000985599545984

Publication date: March 1, 1999

More about this publication?
Related content

Tools

Favourites

Share Content

Access Key

Free Content
Free content
New Content
New content
Open Access Content
Open access content
Subscribed Content
Subscribed content
Free Trial Content
Free trial content
UA-1313315-23
Cookie Policy
X
Cookie Policy
ingentaconnect website makes use of cookies so as to keep track of data that you have filled in. I am Happy with this Find out more