Nanostructured Fe50Ni50 alloy prepared by mechanical alloying: synthesis and characterisation

Authors: Adzir, Y.1; Yaacob, I.I.2

Source: Materials Research Innovations, Volume 13, Number 3, September 2009 , pp. 217-220(4)

Publisher: Maney Publishing

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Abstract:

Nanocrystalline Fe50Ni50 alloy was successfully prepared by the mechanical alloying process using planetary high energy ball mill. Fe and Ni elemental powder were milled for various times up to 48 h. The alloy formation and its physical properties were investigated by X-ray diffraction (XRD) technique, scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) analysis. The magnetic properties of the alloy were determined by alternating gradient magnetometer (AGM). Mechanical treatment influenced the physical properties of the alloys by decreasing the crystallite size from 132·21 to 15·08 nm. Results of AGM indicated that the alloying process influenced the magnetic properties of the materials.

Keywords: Fe-NI ALLOY; MECHANICAL ALLOYING; NANOSTRUCTURE; MAGNETIC MEASUREMENT

Document Type: Research article

DOI: 10.1179/143307509X440343

Affiliations: 1: Center for Nanotechnology, Precision and Advanced Materials, Universiti Malaya, 50603 Kuala Lumpur, Malaysia 2: Center for Nanotechnology, Precision and Advanced Materials, Universiti Malaya, 50603 Kuala Lumpur, Malaysia;, Email: iskandar@um.edu.my

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