RFDR with Adiabatic Inversion Pulses: Application to Internuclear Distance Measurements
Source: Journal of Biomolecular NMR, Volume 28, Number 3, March 2004 , pp. 229-233(5)
Abstract:In the context of the structural characterisation of biomolecular systems via MAS solid state NMR, the potential utility of homonuclear dipolar recoupling with adiabatic inversion pulses has been assessed via numerical simulations and experimental measurements. The results obtained suggest that it is possible to obtain reliable estimates of internuclear distances via an analysis of the initial cross-peak intensity buildup curves generated from two-dimensional adiabatic inversion pulse driven longitudinal magnetisation exchange experiments.
Document Type: Research Article
Affiliations: 1: Abteilung Molekulare Biophysik/NMR-Spektroskopie, Institut für Molekulare Biotechnologie, 07745 Jena, Germany 2: Abteilung Molekulare Biophysik/NMR-Spektroskopie, Institut für Molekulare Biotechnologie, 07745 Jena, Germany, Email: firstname.lastname@example.org
Publication date: March 1, 2004