Quantitative Gas Chromatography of Insect Repellent Mixture M-19601

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The repellents in the M-1960 clothing impregnant are 2-butyl- 2-ethyl-l, 3-propane dial, N-butylacetanilide, and benzyl benzoate. They can be analyzed quantitatively by gas chromatography on an 8-foot column of 5% Dow-Corning Silicone 550 on Haloport-F using a thermal conductivity detector. Analyses are conducted at 225 . on as little as 200 micrograms of each repellent, about 15 minutes being required for a single run. An internal standard is included to eliminate error, owing to sample injection.

Document Type: Research Article

Publication date: August 1, 1962

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  • Journal of Economic Entomology is published bimonthly in February, April, June, August, October, and December. The journal publishes articles on the economic significance of insects and is divided into the following sections: apiculture & social insects; arthropods in relation to plant disease; forum; insecticide resistance and resistance management; ecotoxicology; biological and microbial control; ecology and behavior; sampling and biostatistics; household and structural insects; medical entomology; molecular entomology; veterinary entomology; forest entomology; horticultural entomology; field and forage crops, and small grains; stored-product; commodity treatment and quarantine entomology; and plant resistance. In addition to research papers, Journal of Economic Entomology publishes Letters to the Editor, interpretive articles in a Forum section, Short Communications, Rapid Communications, and Book Reviews.
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