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Open Access Preparation and Luminescence Properties of PbF2:Er3+,Yb3+ Up-conversion Light-emitting Materials

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Abstract:

Er3+, Yb3+ co-doped PbF2(PbF2:Er3+,Yb3+) matrix up-conversion luminescence materials were prepared by a hydrothermal method with the NaF and NH4HF2 as fluorine source. A bright green light appears under 1 064 nm laser excitation at room temperature. The phase and morphology of the materials were characterized by scanning electron microscopy and X-ray diffraction, respectively. The influences of annealing temperature and rare earth ions Er3+/Yb3+doping mole ratio on the up-conversion luminescence of PbF2:Er3+,Yb3+ sample were investigated. The results show that the PbF2:Er3+,Yb3+ sample has a greater luminescence intensity when the annealing temperature and reaction time are 550 and 48 h. The optimum luminescence properties of the PbF2:Er3+,Yb3+ sample prepared can be obtained when the doping mole ratio of Er3+/Yb3+ ions is 1:9.

Keywords: hydrothermal method; lead fluoride; rare earth doped fluoride; up-conversion luminescence

Document Type: Research Article

DOI: https://doi.org/10.7521/j.issn.0454-5648.2013.12.22

Affiliations: College of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China

Publication date: 2013-12-01

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  • Journal of the Chinese Ceramic Society (JCCS), published in Chinese and in English, is a comprehensive monthly periodical focused on the fields of inorganic and non-metallic materials. The main purpose of the JCCS is to report the latest creative achievements in research, production and design for ceramics, glass, cementing materials, refractory, artificial crystals and other non-metallic materials. JCCS is regarded as an important journal in inorganic and non-metallic materials sciences in China and has been awarded by China Association for Science and Technology. The full-text of papers in JCCS is also published by CNKI (China National Knowledge Infrastructure). JCCS is indexed in EI Compendex, CA( Chemical Abstracts) ,SA and Ж and more than 20 databases.
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