Skip to main content

Characterization of Undigested Particulate Material Following Microwave Digestion of Recycled Document Papers

Buy Article:

$43.00 plus tax (Refund Policy)


Recycled document paper was microwave digested in a solution of HNO3 and H2O2 prior to analysis by inductively coupled plasma mass spectrometry (ICP-MS) to determine the trace elemental concentrations within the paper. Undigested particulate material was observed and subsequently characterized as a mixture of kaolin (clay) and TiO2 by Fourier transform infrared spectroscopy and X-ray diffraction spectroscopy. The effect of the particulate material on the elemental concentrations was then investigated. Paper samples were completely digested in hydrofluoric acid (HF) and element concentrations determined in the HF and HNO3/H2O digests were statistically compared using Student’s t-test (95% confidence limit). Statistical differences in element concentrations between the two digests were observed for only four elements and there was no evidence of element adsorption by the particulate material. Hence, the HNO3/H2O2 digestion proved sufficient to digest paper for ICP-MS analysis, eliminating the need to use the hazardous and corrosive HF matrix.
No References
No Citations
No Supplementary Data
No Article Media
No Metrics

Keywords: document paper; forensic science; inductively coupled plasma mass spectrometry; microwave digestion; trace elements; undigested particulate material

Document Type: Research Article

Affiliations: 1: Forensic Science Program, School of Criminal Justice, Michigan State University, East Lansing, MI. 2: Department of Geological Sciences, Michigan State University, East Lansing, MI.

Publication date: 2009-09-01

  • Access Key
  • Free content
  • Partial Free content
  • New content
  • Open access content
  • Partial Open access content
  • Subscribed content
  • Partial Subscribed content
  • Free trial content
Cookie Policy
Cookie Policy
Ingenta Connect website makes use of cookies so as to keep track of data that you have filled in. I am Happy with this Find out more