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Reconstruction of the Cubic and Tetragonal Parent Grains from Electron Backscatter Diffraction Maps of Monoclinic Zirconia

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Abstract:

Monoclinic zirconia results from cubic→tetragonal→monoclinic phase transformations occurring at high temperature. Electron backscatter diffraction maps of monoclinic zirconia in fused-cast refractories have been treated with new crystallographic computer programs. The correct orientation relationships between the three phases have been identified among those proposed in the literature, the tetragonal and cubic parent grains have been automatically reconstructed, and the variants have been indexed. This example illustrates the possibilities of automatic crystallographic reconstruction software to study complex phase transition materials.

Document Type: Research Article

DOI: https://doi.org/10.1111/j.1551-2916.2010.03894.x

Affiliations: 1: CEA, LITEN, DEHT, Minatec, 38054 Grenoble, France 2: Université de Lyon, INSA-Lyon, 69021 Villeurbanne, France 3: Ecole des Mines de Saint-Etienne, 42023 Saint-Etienne, France

Publication date: 2010-09-01

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