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In Situ Study of the Reaction Sequence in the Sol–Gel Synthesis of a (Ba0.5Sr0.5)(Co0.8Fe0.2)O3− Perovskite by X-Ray Diffraction and Transmission Electron Microscopy

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Abstract:

Examination of the complexing citric acid/EDTA synthesis of (Ba0.5Sr0.5)(Co0.8Fe0.2)O3− is presented by in situ X-ray diffraction and transmission electron microscopy, which elucidate all intermediate phases and the formation of the perovskite structure for the first time.

Document Type: Research Article

DOI: http://dx.doi.org/10.1111/j.1551-2916.2007.01932.x

Affiliations: Institute of Physical Chemistry and Electrochemistry, Leibniz Universit├Ąt Hannover, D-30167 Hannover, Germany

Publication date: November 1, 2007

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