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DADD-Assisted Hydrothermal Synthesis of t-ZrO2 Nanoparticles

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Tetragonal ZrO2 (t-ZrO2) nanoparticles (diameter: ca. 10 nm; BET-specific surface area: 100 m2/g) are hydrothermally prepared via crystallization of 1,12-diaminododecane (DADD)-hydrous zirconia gels at 230°C for 3 days. The volume content of monoclinic phase is ca. 0.1. The surface-adsorbed hydrocarbon layer (ca. 3 wt%) is observed by FTIR and TGA. They account for the formation of our t-ZrO2 nanoparticles with high-phase purity.
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Document Type: Research Article

Affiliations: 1: Chemical and Process Engineering Center, National University of Singapore, Singapore 117576, Singapore 2: Department of Chemistry, National University of Singapore, Singapore 117543, Singapore 3: Department of Chemical and Environment Engineering, National University of Singapore, Singapore 119260, Singapore

Publication date: 2005-09-01

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