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Bis(1,10-phenanthroline-2N,N′)(squarato-O)copper(II) trihydrate

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Abstract:

The title mononuclear [Cu(sq)(phen)2]·3H2O complex [sq is squarate (C4O4) and phen is 1,10-phenanthroline (C12H8N2)] has been synthesized and the structure consists of a neutral mononuclear [Cu(sq)(phen)2] unit and three solvate water mol­ecules. The CuII ion has distorted square-pyramidal coordination geometry, comprised of one carboxyl­ate O atom from a monodentate squarate ligand and four N atoms from two chelating phen ligands. An extensive three-dimensional network of OW—H…O/OW hydrogen bonds, face-to-face –­ interactions between the 1,10-phenanthroline aromatic rings and a weak –ring interaction are responsible for crystal stabilization.

Document Type: Research Article

DOI: http://dx.doi.org/10.1107/S0108270104020566

Publication date: October 1, 2004

bsc/ayc/2004/00000060/00000010/art00022
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