Detailed example of the identification and crystallographic analysis of a pseudo‐merohedrally twinned crystal
Authors: Guzei, Ilia; Herbst‐Irmer, Regine; Munyaneza, Apollinaire; Darkwa, James
Source: Acta Crystallographica Section B, Volume 68, Number 2, 1 April 2012 , pp. 150-157(8)
Abstract:A detailed description of the procedures utilized in the non‐routine X‐ray single‐crystal structural determination and refinement of a pseudo‐merohedrally twinned crystal of an Fe/Ni organometallic complex is presented. It illustrates to the practitioners of crystallography how to properly handle such cases and describes the logic and concrete steps necessary to account for the twinning, pseudo‐symmetry and atomic positional disorder.
Document Type: Research Article
Publication date: April 1, 2012