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Mild, Efficient and Highly Selective Hydrolysis of Acetonides with Antimony Trichloride(SUPPORTING INFORMATION)

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A mild and efficient procedure for chemoselective and regioselective hydrolysis of acetonide with SbCl3 in the presence of other frequently used hydroxy protecting groups, TBDMS, TBDPS, Bz, Bn, Ac, Ts and Tr, was described. The mechanism was examined and proposed.

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Keywords: Hydrolysis; acetonide; antimony; catalysis; lewis acid; protecting groups

Document Type: Research Article

Affiliations: Dept. of Appl. Chem. Beijing Institute of Technology, Beijing 100081, China.

Publication date: 2006-04-01

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  • Letters in Organic Chemistry publishes original letters on all areas of organic chemistry including synthesis, bioorganic, medicinal, natural products, organometallic, supramolecular, molecular recognition and physical organic chemistry. The emphasis is placed on publishing quality papers very rapidly. Letters are processed rapidly and take full advantage of the Internet technology both for the submission and the review of the manuscripts.
    The journal is essential reading for all organic chemists both in academia and industry.
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