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Characteristics of Nano-Sized (Pb, La)TiO3 Powder Synthesized at Room Temperature

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We synthesized nano-sized (Pb, La)TiO3 powder using a high energy mechano-chemical technique at room temperature. By the results, nano-sized (Pb, La)TiO3 powder with perovskite structure was successfully synthesized from an oxide mixture using a high energy mechano-chemical technique without any post-annealing. The mechanically-synthesized (Pb, La)TiO3 powder consisted of nanometer sized particles and had very high homogeneity. According to increase of milling time, source phases such as Pb oxides and TiO2 disappeared and the perovskite PLT phase was formed by chemical reaction and the release of OH group.
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Keywords: (PB, LA)TIO3; HIGH ENERGY MECHANO-CHEMICAL TECHNIQUE; MILLING TIME; XAS; XPS

Document Type: Research Article

Publication date: 2012-02-01

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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