Preparation of SnO2 Nanowires by Solvent-Free Method Using Mesoporous Silica Template and Their Gas Sensitive Properties

Authors: Zhang, Haijiao; Tan, Zhijin; Xu, Panpan; Oh, Kokyo; Wu, Ruofei; Shi, Wenming; Jiao, Zheng

Source: Journal of Nanoscience and Nanotechnology, Volume 11, Number 12, December 2011 , pp. 11114-11118(5)

Publisher: American Scientific Publishers

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Abstract:

In this paper, a facile method was presented to synthesize tin dioxide (SnO2) nanowires by solventfree method using SnCl2·2H2O as precursor and mesoporous silica SBA-15 as the hard template. No solvent was used in the processing. The products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS) and N2 adsorption/desorption isotherms. The results indicated that SnO2 nanowires fabricated by this method have a diameter of about 8 nm and a relatively high surface area 73.0 m2/g. The gas sensing properties of SnO2 nanowires were measured. The response and recovery time of this sensor were 6 s and 12 s, respectively. With the concentration of toluene increasing, the response of the sensor doubled increase. Compared with bulk SnO2, SnO2 nanowires showed much higher response to toluene.

Keywords: SNO2 NANOWIRES; MESOPOROUS SILICA TEMPLATE; GAS SENSORS; SOLVENT-FREE

Document Type: Research article

DOI: http://dx.doi.org/10.1166/jnn.2011.3978

Publication date: 2011-12-01

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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