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Synthesis of Silver Nanoparticles by Oleylamine-Oleic Acid Reduction and Its Use in Making Nanocable by Coaxial Electrospinning

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In the present study, silver nanoparticles were produced by hydrazine hydrate and oleylamine/oleic acid systems in order to investigate the effects of reducing agents with different strengths on the reduction mechanism. Particle size and size distribution of silver particles produced by slow reducing system were studied in detail by using transmission electron microscopy (TEM), X-Ray Diffraction (XRD), photon correlation spectroscopy (PCS), and surface plasmon resonance spectroscopy (SPR). Finally, reduction mechanism by oleylamine and oleic acid system was clarified and particles with average diameter of 2.7 nm were produced. Nano-sized particles were then placed at the center of the polymer fibers by coaxial electrospinning and nanocable like structures were produced. SEM and TEM were used for the characterization of these cables.
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Keywords: ELECTROSPINNING; HYDRAZINE HYDRATE; METAL NANOPARTICLE; METAL/POLYMER NANOCOMPOSITE; NANOCABLE; OLEIC ACID; OLEYLAMINE; SILVER

Document Type: Research Article

Publication date: 2011-04-01

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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