Crystallite Sizes and Lattice Parameters of Nano-Biomagnetite Particles

Authors: Moon, Ji-Won; Rawn, Claudia J.; Rondinone, Adam J.; Wang, Wei; Vali, Hajatollah; Yeary, Lucas W.; Love, Lonnie J.; Kirkham, Melanie J.; Gu, Baohua; Phelps, Tommy J.

Source: Journal of Nanoscience and Nanotechnology, Volume 10, Number 12, December 2010 , pp. 8298-8306(9)

Publisher: American Scientific Publishers

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Abstract:

Average crystallite sizes of microbially synthesized pure, metal-, and lanthanide-substituted magnetite (bio-magnetite) were determined for a variety of incubation times and temperatures, substitutional elements and amounts, bacterial species, and precursor types. The intriguing difference between nanoparticle bio-magnetite and chemically synthesized magnetite (chem-magnetite) was that powder X-ray diffraction (XRD) data showed that the bio-magnetite exhibited slightly smaller lattice parameters, however, Raman Spectroscopy exhibited no difference in Fe–O bonding. These results indicate that bio-magnetite likely exhibits a more compact crystal structure with less uncoordinated iron on the surface suppressing negative pressure effects. The bio-magnetite with decreased lattice parameters could have potential technological advantages over current commercial chemically synthesized magnetites.

Keywords: CRYSTALLITE SIZE; LATTICE PARAMETERS; MAGNETITE; MICROBIAL SYNTHESIS

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2010.2745

Publication date: December 1, 2010

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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