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Controlled Synthesis and Characterization of ZnSe Quantum Dots

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Abstract:

Adopting improved metal-organic "Green method," Colloidal ZnSe quantum dots were synthesized by using cheap and low toxic zinc oxide (ZnO) in an organic solvent system of 1-hexadecylamine (HDA), lauric acid (LA) and tri-n-octylphosphine (TOP). The effects of HDA dosage, injection temperature, growth temperature and time on the microstructure and optical properties of ZnSe were studied by means of X-Ray diffraction(XRD), transmission electron microscopy (TEM), spectrofluorometers and ultraviolet spectrophotometer, respectively. The results showed that ZnSe quantum dots with the best range of the size evolution were obtained under the condition of injection at 280 °C and growth at 240 °C by choosing the optimal parameters of ZnO:HDA:LA = 1:2.1:5.2 and TOPSe = 1 mol/L. Its size became larger and the emission peak shifted obviously to red with increasing the growth time. Meanwhile, the obtained ZnSe was of the wurtzite structure, had good uniformity and fluorescent characteristics.

Keywords: CONTROLLED SYNTHESIS; OPTICAL PROPERTIES; ZNSE QUANTUM DOTS

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2010.2905

Publication date: November 1, 2010

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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