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Synthesis of Sb2E3 (E = S, Se) Nanorods with a Flat Cross Section by a Rapid Hot Injection Method

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Abstract:

We report herein a simple colloidal synthesis route, i.e., rapid injection of E (E = S, Se) source into a hot solvent (1-octadecence, ODE) containing antimony precursor (antimony stearate), to grow Sb2E3 nanorods. The as-prepared nanorods were extensively characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and high-resolution transmission electron microscopy (HRTEM). The mechanism for growth of Sb2E3 nanorods was also clarified from the view of crystal structure-directed growth. We believe that the method present here is a more straightforward and costeffective route to prepare Sb2E3 nanocrystals with high quality.

Keywords: CRYSTAL GROWTH; ONE-DIMENSION NANOSTRUCTURES; SB2S3 NANOCRYSTALS; SB2SE3 NANOCRYSTALS; SHAPE-CONTROLLED SYNTHESIS

Document Type: Research Article

DOI: https://doi.org/10.1166/jnn.2010.2871

Publication date: 2010-11-01

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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