Skip to main content

Preparation and Thermal-Mechanical Characterization of Nanoclay-Unsaturated Polyester Composites

Buy Article:

$105.00 plus tax (Refund Policy)

Recently polymer nanocomposites have attracted great interest as much as in industry as in research laboratories, due to they often show remarkable improvement in their mechanical and thermal properties when are compared with the virgin polymers. Among nanocomposites, nanoclayreinforced polymers have been widely studied, specifically, those formed by a thermosetting polymer matrix, like unsaturated polyester crosslinked resin reinforced with layered silicates, like montmorillonite. In this work we have prepared nanocomposites formed by an isophtalic unsaturated polyester crosslinked resin (UP) reinforced with different contents (2–10 wt%) of organic modified montmorillonite (OMMT). The UP/OMMT nanocomposites have been prepared following different procedures and the structural characterization has been carried out by using X-ray diffraction (XRD). In all the cases an increase of the d-spacing between layers of the OMMT has been detected. The objective of this study is to analyze the thermal and mechanical behaviour of nanocomposites. For all of the reinforced systems, the glass transition temperatures values, Tg, obtained by differential scanning calorimetry (DSC) and dynamic-mechanical thermal analysis, (DMTA) are higher than the corresponding ones to neat UP. On the other hand, the OMMTP mechanical behaviour has been evaluated by DMTA and by tensile tests. Both techniques reveal an increase in Young modulus, however, a decrease of the tensile strength is observed in all the reinforced systems.
No Reference information available - sign in for access.
No Citation information available - sign in for access.
No Supplementary Data.
No Article Media
No Metrics


Document Type: Research Article

Publication date: 2010-04-01

More about this publication?
  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
  • Editorial Board
  • Information for Authors
  • Subscribe to this Title
  • Terms & Conditions
  • Ingenta Connect is not responsible for the content or availability of external websites
  • Access Key
  • Free content
  • Partial Free content
  • New content
  • Open access content
  • Partial Open access content
  • Subscribed content
  • Partial Subscribed content
  • Free trial content
Cookie Policy
Cookie Policy
Ingenta Connect website makes use of cookies so as to keep track of data that you have filled in. I am Happy with this Find out more