ZnO Hierarchical Nanostructures: Simple Solvothermal Synthesis and Growth Mechanism

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Abstract:

Hierarchical nano/micro structures of ZnO have been fabricated by solvothermal approach on sol–gel derived ZnO thin films. Paintbrush like nano/micro rod assembly, double-sided brush and windmill type architectures of ZnO are obtained when the ZnO thin film coated substrates were treated solvothermally in water at pH 10. Aligned nanorods are obtained at pH ∼ 13.5 in water. In ethylenediamine-water solvent divergent micro/nanorod assemblies such as hemispherical dandelion, rice plant type bush of ZnO are obtained. Increase in the percentage of ethyelendiamine resulted in the formation of smaller assemblies of relatively thin nanorods. Initial slow reaction caused by the slow increase of the temperature inside the reaction medium and the different growth kinetics of the ZnO crystals are supposed to be the reason behind the architectural assemblies of the ZnO crystals.

Keywords: NANO AND MICRO STRUCTURE; SCANNING AND TRANSMISSION ELECTRON MICROSCOPY; ZINC OXIDE

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2008.333

Publication date: September 1, 2008

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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