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Sonochemical Reaction of Fullerene[C60] with Several 2′-Azidoethyl per-O-Acetyl Glycosides

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Abstract:

Cycloadditive reaction of fullerene[C60] with various 2′-azidoethyl per-O-acetyl glycopyranoside of D-mannose, D-galactose, D-glucose, D-xylose and D-maltose, respectively gave the glycosyl fullerene[C60] derivatives 2a–2e such as α-D-mannosyl fullerene[C60] under ultrasonication. Based on analyses using 1H- and 13C-NMR, UV-vis, FT-IR, and FAB-MS spectroscopies of the glycosyl fullerene[C60] derivatives, the products were composed of a mixture of [5,6]- and [6,6]-junction isomers which were predominantly the closed [5,6]-junction isomer.

Keywords: 2′-AZIDOETHYL PER-O-ACETYL GLYCOSIDES; CYCLOADDITIVE REACTION; FULLERENE[C60]; ULTRASONICATION

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2008.091

Publication date: June 1, 2008

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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