Sonochemical Reaction of Fullerene[C60] with Several 2′-Azidoethyl per-O-Acetyl Glycosides
Authors: Yoon, Shinsook; Ho Hwang, Sung; Bae Ko, Weon
Source: Journal of Nanoscience and Nanotechnology, Volume 8, Number 6, June 2008 , pp. 3136-3141(6)
Publisher: American Scientific Publishers
Abstract:Cycloadditive reaction of fullerene[C60] with various 2′-azidoethyl per-O-acetyl glycopyranoside of D-mannose, D-galactose, D-glucose, D-xylose and D-maltose, respectively gave the glycosyl fullerene[C60] derivatives 2a–2e such as α-D-mannosyl fullerene[C60] under ultrasonication. Based on analyses using 1H- and 13C-NMR, UV-vis, FT-IR, and FAB-MS spectroscopies of the glycosyl fullerene[C60] derivatives, the products were composed of a mixture of [5,6]- and [6,6]-junction isomers which were predominantly the closed [5,6]-junction isomer.
Document Type: Research Article
Publication date: June 1, 2008
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