Sonochemical Reaction of Fullerene[C60] with Several 2′-Azidoethyl per-O-Acetyl Glycosides
Abstract:Cycloadditive reaction of fullerene[C60] with various 2′-azidoethyl per-O-acetyl glycopyranoside of D-mannose, D-galactose, D-glucose, D-xylose and D-maltose, respectively gave the glycosyl fullerene[C60] derivatives 2a–2e such as α-D-mannosyl fullerene[C60] under ultrasonication. Based on analyses using 1H- and 13C-NMR, UV-vis, FT-IR, and FAB-MS spectroscopies of the glycosyl fullerene[C60] derivatives, the products were composed of a mixture of [5,6]- and [6,6]-junction isomers which were predominantly the closed [5,6]-junction isomer.
Document Type: Research Article
Publication date: June 1, 2008
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