Growth of Zinc Oxide Nanorods, Tetrapods, and Nanobelts without Catalyst

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Abstract:

Zinc oxide (ZnO) nanostructures with various morphologies have been synthesized without catalyst in a one-step simple redox process. The results show that ZnO nanorods, nanobelts, and tetrapods with hexagonal needled arms could be synthesized via thermal treatment of a mixture of zinc oxide and charcoal powder in a muffle furnace at 1000–1200 °C for 240 min. XRD analyses showed that polycrystalline ZnO phase with wurtzite crystal structure was formed. At a relatively low temperature, 1000 °C, the ZnO structure was found to be a bundle of denser nanorods. By increasing the reaction temperature to 1100 °C, tetrapod-like structures of needle-like arms with pyramidal tips were formed. With the increase of temperature up to 1200 °C, the morphology of ZnO nanostructures changed from nanorods and tetrapods to coalescence grains. Reaction temperature was found to be the most important experimental parameter that played an important role in controlling the mode, mechanism of growth, and formation of different ZnO morphologies.

Keywords: NANOBELTS; SYNTHESIS; TETRAPODS; ZNO NANORODS

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2006.355

Publication date: July 1, 2006

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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