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Preparation of AlFe Nanoparticles by Mechanical Alloyed Technique

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Small metallic particles (1–3 nm) have been obtained using mechanical alloying techniques. Analytical techniques such as scanning electron microscopy have been used for the morphological and chemical characterization of the AlFe alloyed powders. B, Ni and Ti have been explored as reinforced elements to the initial AlFe mixture. X-ray diffraction patterns and transmission electron microscopy (TEM) techniques have been employed for the structural characterization of the small metallic particles. Theoretical simulations based on molecular dynamics have been used to interpret some of the experimental structural results. Furthermore, theoretical simulations of HREM images based on the dynamical theory of electron diffraction have also been obtained and comparisons with the experimental results have been carried out. The complementary analyses determined that the produced clusters are basically AlFe alloyed nanoparticles immersed in a matrix and with multiple defected structures.
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Keywords: ALFE NANOPARTICLES; BIMETALLIC CLUSTER; ELECTRON MICROSCOPY; MECHANOCHEMISTRY; MOLECULAR SIMULATIONS

Document Type: Research Article

Publication date: 2005-12-01

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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