Synthesis and Thermal Behaviour of Nanostructured ZrO2 Powders Obtained Under Hydrothermal Conditions

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Abstract:

Nanocrystalline zircone (ZrO2) powders were synthesized from zirconium oxyacetate aqueous solution treated up to 240 °C under autogeneous pressure. Depending on experimental conditions, colloidal particles of 26–150 nm are formed by aggregation of zirconia crystallites. The effect of some experimental conditions over the colloidal particle size or zirconia phase composition was studied. The powder sintering behaviour is also presented.

Keywords: COLLOIDAL PARTICLES; HYDROTHERMAL SYNTHESIS; SINTERING; ZRO2 NANOSTRUCTURED POWDER

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2005.179

Publication date: October 1, 2005

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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