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A Simple and Versatile Sol–Gel Method for the Synthesis of Functional Nanocrystalline Oxides

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Abstract:

MxOy nanometric powders (Nb2O5, In2O3, and ZrO2) have been efficiently synthesized at low temperatures with the use of simple precursors and with no acid or base catalysis or stabilizing agents. The powdershave been characterized by Thermogravimetry/Differential Thermal Analysis, X-ray diffraction, and scanning electron microscopy. The oxides obtained have well-defined crystalline structures, exhibit homogeneity, and crystallite sizes ranging from 9 to 16 nm in diameter.

Keywords: NANOCRYSTALLINE OXIDES; SEM; SOL-GEL METHOD; THERMAL METHODS; XRD

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2005.072

Publication date: April 1, 2005

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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