Synthesis of Solvent-Stabilized Colloidal Nanoparticles of Platinum, Rhodium, and Rutheniumby Microwave-Polyol Process

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Abstract:

Solvent-stabilized Pt, Rh, and Ru colloidal nanoparticles were synthesized by a microwave-polyol process. They were characterized by TEM and XPS, XRD, and UV–vis examination. These colloids have small particle sizes with narrow size distribution, and they were stable in glycol upon storage under ambient condition for months. Separation and XPS characterization of the intermediate col- loids demonstrated the two-step mechanism for the formation of solvent-stabilized metal colloids via hydrolysis.

Keywords: GLYCOL; MICROWAVE; PLATINUM; RHODIUM; RUTHENIUM; SOLVENT-STABILIZED NANOPARTICLES

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/jnn.2005.028

Publication date: February 1, 2005

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  • Journal for Nanoscience and Nanotechnology (JNN) is an international and multidisciplinary peer-reviewed journal with a wide-ranging coverage, consolidating research activities in all areas of nanoscience and nanotechnology into a single and unique reference source. JNN is the first cross-disciplinary journal to publish original full research articles, rapid communications of important new scientific and technological findings, timely state-of-the-art reviews with author's photo and short biography, and current research news encompassing the fundamental and applied research in all disciplines of science, engineering and medicine.
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