Synthesis and Characterization of CdS Microflowers

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Abstract:

In this manuscript, we have reported a template free fabrication of CdS microflowers by the thermal decomposition of cadmium thiocyanate complex at 300 °C under open atmospheric condition. This synthetic methodology opens a new window for a well crystallized, single phase CdS preparation in large-scale. The formation of microflower morphology was investigated under various experimental conditions and the results imply that the decomposition temperature, co-solvents, cadmium and sulfur precursors played an important role on the formation of microflower morphology. The synthesized CdS has been characterized by using XRD, XPS, FE-SEM and HR-TEM. The XRD patterns revealed that the formation of pure wurtzite phase at all decomposition temperature and the XPS results also confirmed the formation of CdS. The FE-SEM picture indicated that the microflower morphology was self-assembled by the intact of thin nano-sheets. A plausible mechanism of CdS microflower formation has been discussed on the basis of the experimental results.

Document Type: Research Article

DOI: http://dx.doi.org/10.1166/asl.2010.1140

Publication date: December 1, 2010

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  • ADVANCED SCIENCE LETTERS is an international peer-reviewed journal with a very wide-ranging coverage, consolidates research activities in all areas of (1) Physical Sciences, (2) Biological Sciences, (3) Mathematical Sciences, (4) Engineering, (5) Computer and Information Sciences, and (6) Geosciences to publish original short communications, full research papers and timely brief (mini) reviews with authors photo and biography encompassing the basic and applied research and current developments in educational aspects of these scientific areas.
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