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First Isolation and Identification of a Di-N-Acyl Derivative of 5,7-Diamino-3,5,7,9-tetradeoxy-L-glycero-D-galacto-non-2-ulosonic (8-Epilegionaminic) Acid

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5,7-Diacetamido-3,5,7,9-tetradeoxy-L-glycero-D-galacto-non-2-ulosonic (di-N-acetyl-8-epilegionaminic) acid was isolated, for the first time, from the O-specific polysaccharide of Escherichia coli O108 by three sequential Smith degradations followed by mild acid hydrolysis of the resultant glycoside. The monosaccharide obtained was identified by a comparison with the synthetic authentic sample using 1H and 13C NMR spectroscopy.
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Document Type: Research Article

Publication date: 2009-09-01

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  • ADVANCED SCIENCE LETTERS is an international peer-reviewed journal with a very wide-ranging coverage, consolidates research activities in all areas of (1) Physical Sciences, (2) Biological Sciences, (3) Mathematical Sciences, (4) Engineering, (5) Computer and Information Sciences, and (6) Geosciences to publish original short communications, full research papers and timely brief (mini) reviews with authors photo and biography encompassing the basic and applied research and current developments in educational aspects of these scientific areas.
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