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Free Content Synthesis of Magnetically Graphitic Mesoporous Carbon from Hard Templates and Its Application in the Adsorption Treatment of Traditional Chinese Medicine Wastewater

Magnetically graphitic mesoporous carbon (Fe/GMC) was synthesized, using SBA-15 as a template and sucrose as a carbon source, with the assistance of ferric nitrate impregnation. The properties of the products were characterized using powder X-ray diffraction (XRD), transmission electron microscopy (TEM), N2 adsorption-desorption (BET), and Raman spectroscopy. The impregnation of Fe3+ promoted the partial graphitization of ordered mesoporous carbon at low temperature (900°), and resulted in the production of magnetic Fe3O4 particles. These complex materials possessed an ordered mesoporous pore structure, large surface area, and magnetic properties. The adsorption properties of Fe/GMC for traditional Chinese medicine wastewater were studied in detail using UV-Vis spectroscopy. The results showed that the Fe/GMC materials displayed rapid adsorption, and had a high adsorption capacity. Fe/GMC could be used as an absorbent for the highly efficient removal of pigments from Carthamus tinctorius flowers via rapid solid-liquid magnetic separation.

Keywords: Graphitization; Hard template; Magnetic Fe3O4; Mesoporous carbon; SBA-15

Document Type: Research Article

Publication date: 15 March 2013

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  • Acta Physico-Chimica Sinica, founded in 1985, is sponsored by the Chinese Chemical Society and organized by the College of Chemistry and Molecular Engineering, PekingUniversity. Since 1997, Acta Physico-Chimica Sinica has been indexed in SCI of ISI (US). Acta Physico-Chimica Sinica is devoted to reporting new and original experimental and theoretical basic research of interest to physical chemists, biophysical chemists, and material physical chemists. Manuscripts that are essentially reporting data, applications of data, or reviews of the literature are not suitable for publication in Acta Physico-Chimica Sinica.
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